C₂₇H₄₃NO₃

Base Information

Chemical Name:C₂₇H₄₃NO₃
CAS No.:1327311-87-4
Molecular Formula:C₂₇H₄₃NO₃
Molecular Weight:429.643
Hs Code.:

C<sub>27</sub>H<sub>43</sub>NO<sub>3</sub>

Synonyms:C₂₇H₄₃NO₃

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Chemical Property of C₂₇H₄₃NO₃

Chemical Property:

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Technology Process of C₂₇H₄₃NO₃

There total 9 articles about C₂₇H₄₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955030-40-7
C₁₄H₂₀O₃

: 1327311-87-4
C₂₇H₄₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / 1 h / -78 °C

2: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 0 - 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; water; tert-butyl alcohol; 1: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.087

Reference yield:

: C₁₂H₂₆O₂Si

: 1327311-87-4
C₂₇H₄₃NO₃

Guidance literature:: Multi-step reaction with 8 steps

1: titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -20 °C

2: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h

3: ethanol; zinc / 3 h / 80 °C

4: sodium hydride / tetrahydrofuran / 14 h / 0 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / 1 h / -78 °C

7: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 0 - 20 °C

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With 1H-imidazole; titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; oxalyl dichloride; ethanol; Cumene hydroperoxide; tetrabutyl ammonium fluoride; iodine; sodium hydride; D-(-)-diisopropyl tartrate; benzotriazol-1-ol; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 1: Sharpless asymmetric epoxidation / 6: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.087

Reference yield:

: 955030-25-8
C₁₄H₁₈O₃

: 1327311-87-4
C₂₇H₄₃NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 0 - 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.06.087