(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

Base Information

Chemical Name:(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide
CAS No.:914983-68-9
Molecular Formula:C₂₂H₁₇F₃N₂O₆
Molecular Weight:462.382
Hs Code.:

Synonyms:(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

Suppliers and Price of (2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

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Technology Process of (2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

There total 9 articles about (2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 914983-67-8
C₂₂H₁₉F₃N₂O₇

: 914983-68-9
(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

Guidance literature:: With pyridine; methanesulfonyl chloride; at -18 ℃; for 144h;
DOI:10.1016/j.bmcl.2006.07.086

Reference yield:

: 228399-13-1
2,5-anhydro-4-azido-3,6-di-O-benzoyl-4-deoxy-D-gulose ethylene acetal

: 914983-68-9
(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

Guidance literature:: Multi-step reaction with 5 steps

1: H₂; CHCl₃ / Pd/C / ethanol / 24 h / 20 °C

2: pyridine / CH₂Cl₂ / 72 h / 4 °C

3: aq. HCl; TFA / 72 h / 4 °C

4: NH₂OH*HCl; NaOAc / ethanol / 2 h / 20 °C

5: 59 percent / mesyl chloride; pyridine / 144 h / -18 °C

With pyridine; hydrogenchloride; chloroform; hydroxylamine hydrochloride; hydrogen; sodium acetate; methanesulfonyl chloride; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.07.086

Reference yield:

: Methanesulfonic acid (1R,2R,4R,5R)-4-[1,3]dioxolan-2-yl-3,6-dioxa-bicyclo[3.1.0]hex-2-ylmethyl ester

: 914983-68-9
(2,5-di-O-benzoyl-3-deoxy-3-trifluoroacetamido-β-D-xylofuranosyl)cyanide

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaN₃ / dimethylsulfoxide / 26 h / 108 - 112 °C

1.2: 23 percent / pyridine / 24 h / 20 °C

2.1: H₂; CHCl₃ / Pd/C / ethanol / 24 h / 20 °C

3.1: pyridine / CH₂Cl₂ / 72 h / 4 °C

4.1: aq. HCl; TFA / 72 h / 4 °C

5.1: NH₂OH*HCl; NaOAc / ethanol / 2 h / 20 °C

6.1: 59 percent / mesyl chloride; pyridine / 144 h / -18 °C

With pyridine; hydrogenchloride; sodium azide; chloroform; hydroxylamine hydrochloride; hydrogen; sodium acetate; methanesulfonyl chloride; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2006.07.086