Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium;

Base Information

• Chemical Name: Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium
• CAS No.: 129576-52-9
• Molecular Formula: CF₃O₃S*C₁₄H₂₃N₂Si
• Molecular Weight: 396.506

Synonyms:Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium;

Chemical Property of Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium;

Chemical Property:

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Technology Process of Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium;

There total 1 articles about Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzylethylenediamine (4152-09-4) → Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium; (129576-52-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / toluene-4-sulfonic acid / 20 h / Heating

2: acetonitrile / 2 h

With toluene-4-sulfonic acid; In acetonitrile;

DOI:10.1039/a802048e

Reference yield: 60.0%

Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium; (129576-52-9) + methacrylonitrile (126-98-7,25067-61-2) → 1-Benzyl-7-methyl-hexahydro-pyrrolo[1,2-a]imidazole-7-carbonitrile (129576-55-2,129576-56-3)

Guidance literature:

With cesium fluoride; In diethylene glycol dimethyl ether;

DOI:10.1016/0040-4039(90)80221-7

Reference yield: 47.0%

Trifluoro-methanesulfonate3-benzyl-1-trimethylsilanylmethyl-4,5-dihydro-3H-imidazol-1-ium; (129576-52-9) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → 1-Benzyl-7-methyl-hexahydro-pyrrolo[1,2-a]imidazole-7-carboxylic acid methyl ester (129576-53-0,129576-54-1)

Guidance literature:

With cesium fluoride; In diethylene glycol dimethyl ether;

DOI:10.1016/0040-4039(90)80221-7

upstream raw materials:

N-benzylethylenediamine

Downstream raw materials:

1-(2-Benzylamino-ethyl)-4,5-dihydro-1H-pyrrole-3-carboxylic acid methyl ester

1-Benzyl-hexahydro-pyrrolo[1,2-a]imidazole-7-carboxylic acid methyl ester

1-Benzyl-7-methyl-hexahydro-pyrrolo[1,2-a]imidazole-7-carboxylic acid methyl ester

1-Benzyl-7-methyl-hexahydro-pyrrolo[1,2-a]imidazole-7-carbonitrile

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