6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

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Chemical Name:6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester
CAS No.:660397-29-5
Molecular Formula:C₆₁H₇₈N₄O₁₇
Molecular Weight:1139.31
Hs Code.:

6-<i>tert</i>-butoxycarbonylamino-hexanoic acid 10-(6-<i>tert</i>-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-<i>tert</i>-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6<i>H</i>-5-oxa-6b-aza-dibenzo[<i>a</i>,<i>i</i>]fluoren-3-yl ester

Synonyms:6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

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Chemical Property of 6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

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Technology Process of 6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

There total 6 articles about 6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 97614-65-8
lamellarin D

: 660397-29-5
6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 23 ℃; for 3h;
DOI:10.1016/j.bmc.2004.01.020

Reference yield: 89.0%

: 660397-29-5
6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

Guidance literature:

Reference yield:

: 6-isopropoxy-7-methoxy-3,4-dihydroisoquinoline

: 660397-29-5
6-tert-butoxycarbonylamino-hexanoic acid 10-(6-tert-butoxycarbonylamino-hexanoyloxy)-13-[4-(6-tert-butoxycarbonylamino-hexanoyloxy)-3-methoxy-phenyl]-2,11-dimethoxy-6-oxo-6H-5-oxa-6b-aza-dibenzo[a,i]fluoren-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,2-dichloro-ethane / 8 h / 23 °C

1.2: 47 percent / DIPEA / 1,2-dichloro-ethane / 32 h / 85 °C

2.1: 94 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CHCl₃ / 2 h / Heating

3.1: 43 percent / AlCl₃ / CH₂Cl₂ / 5.5 h / 23 °C

4.1: 89 percent / EDC*HCl; DMAP / CH₂Cl₂ / 3 h / 23 °C

With dmap; aluminium trichloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; chloroform; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2004.01.020