Technology Process of C38H38O3
There total 7 articles about C38H38O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 8h;
Inert atmosphere;
DOI:10.3762/bjoc.9.132
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
2.1: sodium iodide / acetone / 18 h / Darkness; Reflux; Inert atmosphere
3.1: n-butyllithium; lithium chloride; diisopropylamine / tetrahydrofuran; hexane / 1.33 h / -78 - 20 °C / Inert atmosphere
3.2: 2.5 h / 0 °C / Inert atmosphere
4.1: n-butyllithium; diisopropylamine; borane-ammonia complex / tetrahydrofuran; hexane / 0.83 h / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C / Inert atmosphere
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere
With
n-butyllithium; borane-ammonia complex; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; diisopropylamine; sodium iodide; lithium chloride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; mineral oil;
3.1: |Meyer Alkylation / 3.2: |Meyer Alkylation;
DOI:10.3762/bjoc.9.132
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; diisopropylamine; borane-ammonia complex / tetrahydrofuran; hexane / 0.83 h / 0 - 20 °C / Inert atmosphere
2: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 12 h / 0 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C / Inert atmosphere
With
n-butyllithium; borane-ammonia complex; tetrabutyl ammonium fluoride; sodium hydride; diisopropylamine;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; mineral oil;
DOI:10.3762/bjoc.9.132