(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

Base Information

Chemical Name:(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol
CAS No.:1176030-89-9
Molecular Formula:C₄₅H₆₇NO₄
Molecular Weight:686.031
Hs Code.:

Synonyms:(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

Chemical Property:

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Technology Process of (2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

There total 3 articles about (2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 76-83-5
trityl chloride

: 249728-93-6
(1'S,2'S,3'R)-N-[2,3-dihydroxy-1-(hydroxymethyl)heptadecyl]octanamide

: 1176030-89-9
(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

Guidance literature:: With pyridine; dmap; at 50 ℃;
DOI:10.1016/j.tet.2009.06.007

Reference yield:

: 554-62-1
D-ribo-phytosphingosine

: 1176030-89-9
(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3.5 h / 0 - 20 °C / Inert atmosphere

2: dmap; pyridine / 12 h / 80 °C / Inert atmosphere

With pyridine; dmap; triethylamine; In tetrahydrofuran;
DOI:10.1021/acsmedchemlett.5b00046

Reference yield:

: 111-64-8
n-octanoic acid chloride

: 1176030-89-9
(2S,3S,4R)-2-(N-octanoylamino)-1-O-(triphenylmethyl)-1,3,4-octadecanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3.5 h / 0 - 20 °C / Inert atmosphere

2: dmap; pyridine / 12 h / 80 °C / Inert atmosphere

With pyridine; dmap; triethylamine; In tetrahydrofuran;
DOI:10.1021/acsmedchemlett.5b00046