{2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester

Base Information

• Chemical Name: {2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester
• CAS No.: 851085-36-4
• Molecular Formula: C₃₃H₃₄N₅O₇P
• Molecular Weight: 643.636

Synonyms:{2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester

Chemical Property of {2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester

Chemical Property:

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Technology Process of {2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester

There total 1 articles about {2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzoyl-9-[3'-O-benzoyl-5',6'-dideoxy-6'-(diphenoxyphosphinyl)-2'-C-methyl-β-D-ribohexofuranosyl]adenine (851085-35-3) + benzyl alcohol (100-51-6,185532-71-2) → {2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester (851085-36-4)

Guidance literature:

benzyl alcohol; With sodium hydride;

N⁶-benzoyl-9-[3'-O-benzoyl-5',6'-dideoxy-6'-(diphenoxyphosphinyl)-2'-C-methyl-β-D-ribohexofuranosyl]adenine; In dimethyl sulfoxide; at 20 ℃;

DOI:10.1021/jm049029u

Reference yield:

{2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester (851085-36-4) → {2-[(2R,3R,4R,5R)-5-(6-Amino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester

Guidance literature:

With ammonia; In methanol; at 20 ℃;

DOI:10.1021/jm049029u

Reference yield:

{2-[(2R,3R,4R,5R)-5-(6-Benzoylamino-purin-9-yl)-3,4-dihydroxy-4-methyl-tetrahydro-furan-2-yl]-ethyl}-phosphonic acid dibenzyl ester (851085-36-4) + tert-butyldimethylsilyl chloride (18162-48-6) → N6-benzoyl-9-[5',6'-dideoxy-6'-(dibenzyloxyphosphinyl)-2'-C-methyl-3'-O-tert-butyldimethylsilyl-β-D-ribohexofuranosyl]adenine

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 45 ℃; for 24h;

DOI:10.1021/jm049029u

upstream raw materials:

N⁶-benzoyl-9-[3'-O-benzoyl-5',6'-dideoxy-6'-(diphenoxyphosphinyl)-2'-C-methyl-β-D-ribohexofuranosyl]adenine

benzyl alcohol

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