N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

Base Information

Chemical Name:N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide
CAS No.:161219-95-0
Molecular Formula:C₆₅H₆₄N₄O₉
Molecular Weight:1045.24
Hs Code.:

Synonyms:N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

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Chemical Property of N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

Chemical Property:

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Technology Process of N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

There total 3 articles about N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 68939-45-7
N-(o-Benzyloxy-benzoyl)-glycin

: 74272-81-4
2,3-bis(benzyloxy)-N-(3-(4-(2,3-bis(benzyloxy)benzamido)butylamino)propyl)benzamide

: 161219-95-0
N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

Guidance literature:: With dmap; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C; 2.) rt., 2 d;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 4349-62-6
2-benzyloxybenzoyl chloride

: 161219-95-0
N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

Guidance literature:: Multi-step reaction with 3 steps

2: aq. sodium hydroxide

3: 82 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 68939-33-3
N-(o-Benzyloxy-benzoyl)-glycin-aethylester

: 161219-95-0
N-<3-(2,3-dibenzyl-oxybenzoylamino)propyl>-N-<4-(2,3-dibenzyloxybenzoylamino)-butyl>-2-benzyloxybenzoylglycylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. sodium hydroxide

2: 82 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6