2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester

Base Information

• Chemical Name: 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester
• CAS No.: 882500-05-2
• Molecular Formula: C₁₇H₁₇Cl₂IN₂O₄S
• Molecular Weight: 543.209

Synonyms:2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester

Chemical Property of 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester

Chemical Property:

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Technology Process of 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester

There total 1 articles about 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-amino-5-iodo-isonicotinic acid pentyl ester (882499-88-9) + 2,4-Dichlorobenzenesulfonyl chloride (16271-33-3) → 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester (882500-05-2)

Guidance literature:

With pyridine; In dichloromethane;

Reference yield: 56.0%

4-(piperidine-1-sulfonyl)-benzenethiol (882499-89-0) + 2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester (882500-05-2) → 2-amino-5-[4-(piperidine-1-sulfonyl)-phenylsulfanyl]-isonicotinic acid pentyl ester (882500-06-3)

Guidance literature:

With copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium t-butanolate; In toluene; Heating / reflux;

Reference yield: 29.0%

2-(2,4-dichloro-benzenesulfonylamino)-5-iodo-isonicotinic acid pentyl ester (882500-05-2) + 2,4-Dichlorobenzenesulfonyl chloride (16271-33-3) → 2-(2,4-dichloro-benzenesulfonylamino)-5-[4-(piperidine-1-sulfonyl)-phenylsulfanyl]-isonicotinic acid pentyl ester

Guidance literature:

With pyridine; dmap; at 40 ℃; Product distribution / selectivity;

upstream raw materials:

2-amino-5-iodo-isonicotinic acid pentyl ester

2,4-Dichlorobenzenesulfonyl chloride

Downstream raw materials:

2-amino-5-[4-(piperidine-1-sulfonyl)-phenylsulfanyl]-isonicotinic acid pentyl ester

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