N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

Base Information

Chemical Name:N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide
CAS No.:926649-26-5
Molecular Formula:C₇₆H₁₃₅N₅O₁₁
Molecular Weight:1294.93
Hs Code.:

Synonyms:N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

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Chemical Property of N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

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Technology Process of N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

There total 7 articles about N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 876316-72-2
N,N',N''-tridodecyl-3,3',3''-[(4-carboxyphenyl-carbonylamino)methanetriyl]tripropanamide

: 136586-99-7
4-amino-4-(2-tert-butoxycarbonylethyl)heptanedioic acid di-tertbutyl ester

: 926649-26-5
N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1039/b609645j

Reference yield:

: 883699-81-8
N,N'-didodecyl-4-[3-(dodecylamino)-3-oxopropyl]-4-nitroheptanediamide

: 926649-26-5
N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / H₂ / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr

2.1: SOCl₂; DMF / Heating

2.2: 80 percent / Et₃N / tetrahydrofuran / 40 °C

3.1: 86 percent / aq. KOH / methanol / 5 h / Heating

4.1: 60 percent / DCC; 1-HOBt / CH₂Cl₂ / 96 h / 20 °C

With potassium hydroxide; thionyl chloride; hydrogen; benzotriazol-1-ol; N,N-dimethyl-formamide; dicyclohexyl-carbodiimide; nickel; In methanol; ethanol; dichloromethane;
DOI:10.1039/b609645j

Reference yield:

: 59085-15-3
4-(2-carboxyethyl)-4-nitroheptanedioic acid

: 926649-26-5
N-[tris(2-dodecylaminocarbonyl-ethyl)methyl]-N'-[tris(2-tert-butoxycarbonyl-ethyl)methyl]terephthaldiamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: SOCl; DMF / Heating

1.2: 72 percent / Et₃N / tetrahydrofuran / 96 h / 40 °C

2.1: 88 percent / H₂ / Raney-Ni / ethanol / 24 h / 60 °C / 2625.26 Torr

3.1: SOCl₂; DMF / Heating

3.2: 80 percent / Et₃N / tetrahydrofuran / 40 °C

4.1: 86 percent / aq. KOH / methanol / 5 h / Heating

5.1: 60 percent / DCC; 1-HOBt / CH₂Cl₂ / 96 h / 20 °C

With potassium hydroxide; thionyl chloride; hydrogen; benzotriazol-1-ol; N,N-dimethyl-formamide; dicyclohexyl-carbodiimide; nickel; In methanol; ethanol; dichloromethane;
DOI:10.1039/b609645j