1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

Base Information

Chemical Name:1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline
CAS No.:93757-88-1
Molecular Formula:C₂₂H₂₅NO₉
Molecular Weight:447.442
Hs Code.:

Synonyms:1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

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Chemical Property of 1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

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Technology Process of 1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

There total 6 articles about 1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6702-50-7
3-hydroxy-4-methoxybenzoate

: 93757-85-8
decahydro-2,9-dicarbomethoxy-5,10-epoxy-6-oxoisoquinoline

: 93757-88-1
1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

Guidance literature:: With 18-crown-6 ether; potassium hydride; In tetrahydrofuran; for 40h; Heating;
DOI:10.1021/jo00202a014

Reference yield:

: 645-08-9,74309-78-7
Isovanillic acid

: 93757-88-1
1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / concd. H₂SO₄ / 16 h / Heating

2: 75 percent / KH, 18-crown-6 / tetrahydrofuran / 40 h / Heating

With 18-crown-6 ether; sulfuric acid; potassium hydride; In tetrahydrofuran;
DOI:10.1021/jo00202a014

Reference yield:

: 52805-46-6
2-methoxy-5-cyanophenol

: 93757-88-1
1,2,3,4,6,7,8,9-octahydro-2,9-dicarbomethoxy-5-(2-methoxy-5-carbomethoxyphenoxy)-6-oxoisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / aq. KOH / 6 h / Heating

2: 99 percent / concd. H₂SO₄ / 16 h / Heating

3: 75 percent / KH, 18-crown-6 / tetrahydrofuran / 40 h / Heating

With potassium hydroxide; 18-crown-6 ether; sulfuric acid; potassium hydride; In tetrahydrofuran;
DOI:10.1021/jo00202a014