C₅₄H₈₄O₉Si₂

Base Information

Chemical Name:C₅₄H₈₄O₉Si₂
CAS No.:1381848-84-5
Molecular Formula:C₅₄H₈₄O₉Si₂
Molecular Weight:933.427
Hs Code.:

C<sub>54</sub>H<sub>84</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₅₄H₈₄O₉Si₂

Suppliers and Price of C₅₄H₈₄O₉Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₈₄O₉Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₈₄O₉Si₂

There total 34 articles about C₅₄H₈₄O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1381848-82-3
(2R,4R,6R)-6-((S)-4-((tert-butyldiphenylsilyl)oxy)-2-methyl-3-((triethylsilyl)oxy)butan-2-yl)-2-methoxy-2-(((2S,4S,5S,6S)-6-(2-((4-methoxybenzyl)oxy)ethyl)-5-methyl-4-((triisopropylsilyl)oxy)tetrahydro-2H-pyran-2-yl)methyl)-4-methyldihydro-2H-pyran-3(4H)-one

: 1381848-84-5
C₅₄H₈₄O₉Si₂

Guidance literature:: With camphor-10-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 2.5h;
DOI:10.1021/ol301278e

Reference yield:

: 1381848-71-0
(4R,6R)-6-((S)-4-((tert-butyldiphenylsilyl)oxy)-2-methyl-3-((triethylsilyl)oxy)butan-2-yl)-4-methyltetrahydro-2H-pyran-2-one

: 1381848-84-5
C₅₄H₈₄O₉Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.42 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 0 - 20 °C

2.2: 0.67 h

2.3: 14 h / 20 °C

3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / methanol; dichloromethane / 1.5 h / 0 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 27 h / 0 - 20 °C / Molecular sieve

5.1: camphor-10-sulfonic acid / methanol; dichloromethane / 2.5 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrapropylammonium perruthennate; camphor-10-sulfonic acid; potassium hexamethylsilazane; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ol301278e

Reference yield:

: C₁₈H₂₈O₃Si

: 1381848-84-5
C₅₄H₈₄O₉Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: CrCl(C₆H₂(O)(C₁₀H₁₅)(CH₃)(CHNC₉H₈O)) / 20.5 h / 20 °C / Molecular sieve

2.1: potassium carbonate / methanol / 0.5 h / 20 °C

2.2: 20 °C

3.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.67 h / -20 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

5.1: camphor-10-sulfonic acid / methanol; dichloromethane / 1 h / 0 °C

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 2 h / 20 °C

7.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 2 h / 0 - 20 °C

8.2: 0.67 h

8.3: 14 h / 20 °C

9.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / methanol; dichloromethane / 1.5 h / 0 °C

10.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 27 h / 0 - 20 °C / Molecular sieve

11.1: camphor-10-sulfonic acid / methanol; dichloromethane / 2.5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; sodium tetrahydroborate; tetrapropylammonium perruthennate; CrCl(C₆H₂(O)(C₁₀H₁₅)(CH₃)(CHNC₉H₈O)); cerium(III) chloride heptahydrate; camphor-10-sulfonic acid; potassium tert-butylate; iodine; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol301278e