(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

Base Information

Chemical Name:(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene
CAS No.:91591-11-6
Molecular Formula:C₄₁H₃₇F₃N₂O₁₁
Molecular Weight:790.747
Hs Code.:

(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

Synonyms:(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

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Chemical Property of (1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

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Technology Process of (1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

There total 4 articles about (1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91577-07-0
4-O-benzyl-2,3,6-trideoxy-3-(trifluoroacetamido)-L-lyxohexopyranosyl chloride

: 91593-21-4
(7S,9S)-7,8,9,10-tetrahydro-6,7,9,11-tetrahydroxy-9-<<(phenylcarbamoyl)oxy>methyl>-5,12-naphthacenedione

: 91591-11-6
(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

Guidance literature:: With silver trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether; dichloromethane; at -5 ℃; for 0.5h;
DOI:10.1021/jm00171a011

Reference yield:

: dioxonaphthacene

: 4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 91593-21-4
(7S,9S)-7,8,9,10-tetrahydro-6,7,9,11-tetrahydroxy-9-<<(phenylcarbamoyl)oxy>methyl>-5,12-naphthacenedione

: 91591-11-6
(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

Guidance literature:: In tetrahydrofuran; hexane;

Reference yield:

: 78499-66-8
C₂₇H₂₁BO₈

: 91591-11-6
(1S)-cis-1-[(4-O-benzyl-2,3,6-trideoxy-3-trifluoroacetamido-α-L-lyxohexopyranosyl)oxy]-1,2,3,4,6,11-hexahydro-3,5,12-trihydroxy-6,11-dioxo-3-(phenylcarbamoyloxy)methylnaphthacene

Guidance literature:: Multi-step reaction with 2 steps

2: silver trifluoromethanesulfonate / tetrahydrofuran; CH₂Cl₂; diethyl ether / 0.5 h / -5 °C

With silver trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00171a011