[tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

Base Information

• Chemical Name: [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid
• CAS No.: 470473-77-9
• Molecular Formula: C₂₉H₃₄N₂O₅
• Molecular Weight: 490.599

Synonyms:[tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

Chemical Property of [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

Chemical Property:

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Technology Process of [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

There total 4 articles about [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate (470473-73-5) → [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid (470473-77-9)

Guidance literature:

With lithium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 3h;

DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid (470473-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

2: 82 percent / LiOH / H₂O; dioxane / 3 h / 20 °C

With lithium hydroxide; triethylamine; In 1,4-dioxane; dichloromethane; water;

DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate (172405-21-9) → [tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid (470473-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

2: 82 percent / LiOH / H₂O; dioxane / 3 h / 20 °C

With lithium hydroxide; triethylamine; In 1,4-dioxane; dichloromethane; water;

DOI:10.1016/S0040-4020(02)00527-6

upstream raw materials:

methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

di-tert-butyl dicarbonate

methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

mono-4-methoxytrityl chloride

Downstream raw materials:

[tert-butoxycarbonyl-(2-{2-[tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

[allyloxycarbonyl-(2-{2-[tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid methyl ester

[allyloxycarbonyl-(2-{2-[tert-butoxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-ethyl)-amino]-acetic acid

C₅₅H₇₆N₈O₁₄

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