2-acetylphenyl trichloroacetate

Base Information

• Chemical Name: 2-acetylphenyl trichloroacetate
• CAS No.: 239798-31-3
• Molecular Formula: C₁₀H₇Cl₃O₃
• Molecular Weight: 281.523
• Mol file: 239798-31-3.mol

Synonyms:2-acetylphenyl trichloroacetate

Chemical Property of 2-acetylphenyl trichloroacetate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-acetylphenyl trichloroacetate

There total 1 articles about 2-acetylphenyl trichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-hydroxyacetophenone (118-93-4,104809-67-8) + trifluoroacetyl chloride (76-02-8) → 2-acetylphenyl trichloroacetate (239798-31-3)

Guidance literature:

With pyridine; In tetrahydrofuran; Heating;

DOI:10.1055/s-2002-31966

Reference yield: 70.0%

2-acetylphenyl trichloroacetate (239798-31-3) → o-hydroxyacetophenone (118-93-4,104809-67-8)

Guidance literature:

With [2,2]bipyridinyl; copper(l) chloride; In 1,2-dichloro-ethane; for 1h; Solvent; Schlenk technique; Inert atmosphere; Reflux; Cooling with ice;

DOI:10.1016/j.molstruc.2019.02.018

upstream raw materials:

o-hydroxyacetophenone

trifluoroacetyl chloride

Downstream raw materials:

o-hydroxyacetophenone