(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

Base Information

Chemical Name:(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol
CAS No.:341519-83-3
Molecular Formula:C₃₃H₃₅NO₄Si
Molecular Weight:537.731
Hs Code.:

(2-{4-(<i>tert</i>-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

Synonyms:(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

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Chemical Property of (2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

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Technology Process of (2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

There total 10 articles about (2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 341519-91-3
2,2-dimethyl-propionic acid 2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-benzyl ester

: 341519-83-3
(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran;
DOI:10.3987/com-00-s(i)58

Reference yield:

: 1144-74-7
4-nitrobenzophenone

: 341519-83-3
(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / EtMgBr

2: 78 percent / NaOH; tetrabutylammonium iodide / benzene; H₂O

3: 72 percent / LiEt₃BH / tetrahydrofuran

With sodium hydroxide; ethylmagnesium bromide; tetra-(n-butyl)ammonium iodide; lithium triethylborohydride; In tetrahydrofuran; water; benzene;
DOI:10.3987/com-00-s(i)58

Reference yield:

: 612-14-6
phthalyl alcohol

: 341519-83-3
(2-{4-(tert-butyl-dimethyl-silanyl)-1-[3-methoxy-3-(4-nitro-phenyl)-3-phenyl-prop-1-ynyl]-but-1-en-3-ynyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 9 steps

1: 65 percent / NaH / tetrahydrofuran

2: 79 percent / PDC / CH₂Cl₂

3: tetrahydrofuran

4: CrO₃; H₂SO₄ / acetone

5: 45 percent / Zn / tetrahydrofuran

6: 74 percent / MsCl; Et₃N / CH₂Cl₂

7: 45 percent / EtMgBr

8: 78 percent / NaOH; tetrabutylammonium iodide / benzene; H₂O

9: 72 percent / LiEt₃BH / tetrahydrofuran

With chromium(VI) oxide; sodium hydroxide; dipyridinium dichromate; sulfuric acid; ethylmagnesium bromide; tetra-(n-butyl)ammonium iodide; sodium hydride; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; zinc; In tetrahydrofuran; dichloromethane; water; acetone; benzene;
DOI:10.3987/com-00-s(i)58