(R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

Base Information

Chemical Name:(R)-1-(4-chlorophenyl)-2,2-diethoxyethanol
CAS No.:930278-36-7
Molecular Formula:C₁₂H₁₇ClO₃
Molecular Weight:244.718
Hs Code.:

Synonyms:(R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

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Technology Process of (R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

There total 2 articles about (R)-1-(4-chlorophenyl)-2,2-diethoxyethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 54149-83-6
1-(4-chlorophenyl)-2,2-diethoxyethan-1-one

: 930278-36-7
(R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

Guidance literature:: With C₅₈H₅₆Cl₂N₂P₂Ru; potassium tert-butylate; hydrogen; at 30 ℃; for 4h; under 6080.41 Torr; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/jo801863q

Reference yield:

: 54149-83-6
1-(4-chlorophenyl)-2,2-diethoxyethan-1-one

: (S)-1-(4-chlorophenyl)-2,2-diethoxyethanol

: 930278-36-7
(R)-1-(4-chlorophenyl)-2,2-diethoxyethanol

Guidance literature:: With potassium tert-butylate; hydrogen; RuCl₂[(S)-tolbinap][(R)-dmapen]; In isopropyl alcohol; at 30 ℃; for 4h; under 6080 Torr; Title compound not separated from byproducts;
DOI:10.1021/ol070125+