N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

Base Information

Chemical Name:N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol
CAS No.:124641-27-6
Molecular Formula:C₁₈H₂₁I₂NO₃
Molecular Weight:553.179
Hs Code.:

Synonyms:N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

Chemical Property:

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Technology Process of N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

There total 5 articles about N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.3%

: 124641-26-5
N-[2-Hydroxy-2-(2-iodo-phenyl)-ethyl]-N-(2-iodo-4,5-dimethoxy-benzyl)-formamide

: 124641-27-6
N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

Guidance literature:: With diborane; In tetrahydrofuran; for 1h; Heating;
DOI:10.1248/cpb.37.870

Reference yield:

: 61203-53-0
2-iodo-4,5-dimethoxybenzaldehyde

: 124641-27-6
N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / ethanol / 3 h / Heating

2: NaBH₄ / ethanol / 2 h / Heating

3: 97.3 percent / K₂CO₃, 3 Angstroem molecular sieves / ethanol / 3 h / Heating

4: 69.3 percent / B₂H₆ / tetrahydrofuran / 1 h / Heating

With sodium tetrahydroborate; 3 A molecular sieve; sodium hydrogencarbonate; potassium carbonate; diborane; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.37.870

Reference yield:

: 124641-20-9
β-(2-iodophenyl)ethanolamine

: 124641-27-6
N-(2-iodo-4,5-dimethoxybenzyl)-N-methyl-1-(2-iodophenyl)-2-aminoethanol

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / ethanol / 3 h / Heating

2: NaBH₄ / ethanol / 2 h / Heating

3: 97.3 percent / K₂CO₃, 3 Angstroem molecular sieves / ethanol / 3 h / Heating

4: 69.3 percent / B₂H₆ / tetrahydrofuran / 1 h / Heating

With sodium tetrahydroborate; 3 A molecular sieve; sodium hydrogencarbonate; potassium carbonate; diborane; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.37.870