2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile

Base Information

• Chemical Name: 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile
• CAS No.: 1335032-26-2
• Molecular Formula: C₃₁H₃₂N₆
• Molecular Weight: 488.635

Synonyms:2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile

Chemical Property of 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile

Chemical Property:

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Technology Process of 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile

There total 2 articles about 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-chloro-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile (1335032-41-1) + 4-(2-aminoethyl)-1-(phenylmethyl)piperidine (86945-25-7) → 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile (1335032-26-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; ethanol; for 10h; Reflux;

DOI:10.1016/j.ejmech.2011.05.048

Reference yield:

2,6-dichloro-4-phenylpyridine-3,5-dicarbonitrile (1086-02-8) → 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile (1335032-26-2)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran; ethanol / 5 h / Reflux

2: triethylamine / tetrahydrofuran; ethanol / 10 h / Reflux

With triethylamine; In tetrahydrofuran; ethanol;

DOI:10.1016/j.ejmech.2011.05.048

Reference yield:

2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile (1335032-26-2) → 2-((2-(1-benzylpiperidin-4-yl)ethyl)amino)-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile hydrochloride

Guidance literature:

With hydrogenchloride; In diethyl ether;

DOI:10.1016/j.ejmech.2011.05.048

upstream raw materials:

2-chloro-6-(methyl(prop-2-yn-1-yl)amino)-4-phenylpyridine-3,5-dicarbonitrile

4-(2-aminoethyl)-1-(phenylmethyl)piperidine

2,6-dichloro-4-phenylpyridine-3,5-dicarbonitrile

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