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{(PP3)FeCl}BPh4

Base Information Edit
  • Chemical Name:{(PP3)FeCl}BPh4
  • CAS No.:118933-36-1
  • Molecular Formula:C24H20B*C42H42ClFeP4
  • Molecular Weight:1081.22
  • Hs Code.:
  • Mol file:118933-36-1.mol
{(PP<sub>3</sub>)FeCl}BPh<sub>4</sub>

Synonyms:{(PP3)FeCl}BPh4

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Chemical Property of {(PP3)FeCl}BPh4 Edit
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Technology Process of {(PP3)FeCl}BPh4

There total 2 articles about {(PP3)FeCl}BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; ethanol; N2-atmosphere; stirring FeCl2 (in EtOH) with 1 equiv. phosphine (in THF)for 15 min, addn. of slight excess NaBPh4 (in EtOH), stirring for 15 min; concn., pptn. on EtOH addn., collection (filtration), washing (EtOH, petroleum ether), drying (N2-stream); elem. anal.;
Guidance literature:
With CCl4; byproducts: CHCl3; (N2) or (Ar);
Guidance literature:
With potassium graphite; In toluene; at 20 ℃; for 96h; Inert atmosphere;
DOI:10.1002/ejic.201900058
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