6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

Base Information

Chemical Name:6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid
CAS No.:79705-94-5
Molecular Formula:C₂₄H₂₄BrCl₃O₇
Molecular Weight:610.713
Hs Code.:

Synonyms:6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

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Chemical Property of 6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

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Technology Process of 6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

There total 4 articles about 6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 79705-89-8
1,6-Di-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranose

: 79705-94-5
6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

Guidance literature:: With titanium(IV) bromide; In dichloromethane; ethyl acetate; Ambient temperature;

Reference yield:

: 20771-21-5,51842-23-0,51842-24-1,117561-20-3,125884-32-4,51842-22-9
methyl 2,3-di-O-benzyl-6-O-acetyl-α-D-glucopyranoside

: 79705-94-5
6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / 0.42 h / -20 °C

2: 82 percent / conc. H₂SO₄ / -20 °C

3: 94 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / Ambient temperature

With sulfuric acid; titanium(IV) bromide; In pyridine; dichloromethane; ethyl acetate;

Reference yield:

: 79705-88-7
Methyl-6-O-acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosid

: 79705-94-5
6-O-Acetyl-2,3-di-O-benzyl-4-O-trichloracetyl-α-D-glucopyranosylbromid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / conc. H₂SO₄ / -20 °C

2: 94 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / Ambient temperature

With sulfuric acid; titanium(IV) bromide; In dichloromethane; ethyl acetate;