DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

Base Information

Chemical Name:DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid
CAS No.:338735-77-6
Molecular Formula:C₁₅H₁₅F₃N₄O₅
Molecular Weight:388.303
Hs Code.:

Synonyms:DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

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Technology Process of DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

There total 3 articles about DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 338735-76-5
2-acetylamino-2-{3-[2-nitro-4-(3-trifluoromethyl-3H-diazirin-3-yl)-phenyl]-propyl}-malonic acid

: 338735-77-6
DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

Guidance literature:: In 1,4-dioxane; at 80 ℃; for 1h;
DOI:10.3987/com-00-s(i)90

Reference yield:

: 271252-22-3
3-(azi-2,2,2-trifluoroethyl)-6-(3-bromopropyl)-1-nitrobenzene

: 338735-77-6
DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / NaH / dimethylformamide / 24 h / 20 °C

2: 100 percent / aq. NaOH / ethanol; H₂O / 20 °C

3: dioxane / 1 h / 80 °C

With sodium hydroxide; sodium hydride; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.3987/com-00-s(i)90

Reference yield:

: 338735-74-3
diethyl acetamido[3-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]propyl]malonate

: 338735-77-6
DL-2-acetamido-5-[4-(1-azi-2,2,2-trifluoroethyl)-2-nitrophenyl]pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / aq. NaOH / ethanol; H₂O / 20 °C

2: dioxane / 1 h / 80 °C

With sodium hydroxide; In 1,4-dioxane; ethanol; water;
DOI:10.3987/com-00-s(i)90