Technology Process of propane-2-sulfonic acid {2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]propyl}amide
There total 3 articles about propane-2-sulfonic acid {2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]propyl}amide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium acetate;
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid; sulfuric acid; iodine; periodic acid / water / 3 h / 0 - 60 °C
2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; iodine; potassium acetate; acetic acid; periodic acid;
In
water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; triethylamine / dichloromethane / 16 h / 0 - 20 °C
2: acetic acid; sulfuric acid; iodine; periodic acid / water / 3 h / 0 - 60 °C
3: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 18 h / 80 °C / Inert atmosphere
With
dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; iodine; potassium acetate; acetic acid; periodic acid; triethylamine;
In
dichloromethane; water; N,N-dimethyl-formamide;
