Technology Process of C31H39IO4
There total 6 articles about C31H39IO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; sodium hydrogencarbonate;
In
acetonitrile;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2.1: trimethyl orthoformate / toluene-4-sulfonic acid / methanol / 20 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
3.2: -78 - 20 °C
4.1: tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
5.1: iodine; sodium hydrogencarbonate / acetonitrile / 0.5 h / 20 °C
With
oxalyl dichloride; iodine; sodium hydrogencarbonate; potassium carbonate; dimethyl sulfoxide; trimethyl orthoformate;
toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2.1: trimethyl orthoformate / toluene-4-sulfonic acid / methanol / 20 °C
3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C
3.2: -78 - 20 °C
4.1: tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
5.1: iodine; sodium hydrogencarbonate / acetonitrile / 0.5 h / 20 °C
With
oxalyl dichloride; iodine; sodium hydrogencarbonate; potassium carbonate; dimethyl sulfoxide; trimethyl orthoformate;
toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
