2-acetamidobenzyl diallyl phosphate

Base Information

• Chemical Name: 2-acetamidobenzyl diallyl phosphate
• CAS No.: 494764-01-1
• Molecular Formula: C₁₅H₂₀NO₅P
• Molecular Weight: 325.301
• Mol file: 494764-01-1.mol

Synonyms:2-acetamidobenzyl diallyl phosphate

Chemical Property of 2-acetamidobenzyl diallyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-acetamidobenzyl diallyl phosphate

There total 3 articles about 2-acetamidobenzyl diallyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosphorous acid 2-acetylamino-benzyl ester diallyl ester → 2-acetamidobenzyl diallyl phosphate (494764-01-1)

Guidance literature:

With tert.-butylhydroperoxide; In dichloromethane; acetonitrile; at 20 ℃; for 1.5h;

DOI:10.1139/v02-119

Reference yield:

2-acetamidobenzyl alcohol (20939-77-9) → 2-acetamidobenzyl diallyl phosphate (494764-01-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 2.5 h / 20 °C

2: 190 mg / tert-butyl hydroperoxide / CH₂Cl₂; acetonitrile; various solvent(s) / 1.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; In dichloromethane; acetonitrile;

DOI:10.1139/v02-119

Reference yield:

diallyl diisopropylphosphoramidite (126429-21-8) → 2-acetamidobenzyl diallyl phosphate (494764-01-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 2.5 h / 20 °C

2: 190 mg / tert-butyl hydroperoxide / CH₂Cl₂; acetonitrile; various solvent(s) / 1.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; In dichloromethane; acetonitrile;

DOI:10.1139/v02-119

upstream raw materials:

2-acetamidobenzyl alcohol

diallyl diisopropylphosphoramidite

Refernces