Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid>

Base Information

• Chemical Name: Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid>
• CAS No.: 22435-61-6
• Molecular Formula: C₂₁H₂₂O₆
• Molecular Weight: 370.402

Synonyms:Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid>

Chemical Property of Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid>

Chemical Property:

Purity/Quality:

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Technology Process of Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid>

There total 3 articles about Methyl-2,O³-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

carbon monoxide (201230-82-2) + C21H21IO6 (147577-53-5) → Methyl-2,O3-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid> (22435-61-6) + C22H22O7

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 105 ℃; for 8h; under 62057.8 Torr;

DOI:10.1016/S0040-4039(00)61627-1

Reference yield:

C22H21F3O9S → Methyl-2,O3-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid> (22435-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / NaI / acetone / 6 h / 25 °C

2: Bu₃SnH, AIBN / benzene / 8 h / 105 °C / 62057.8 Torr

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide; In acetone; benzene;

DOI:10.1016/S0040-4039(00)61627-1

Reference yield:

→ Methyl-2,O3-dibenzoyl-4,6-didesoxy-α-D-hexopyranosid> (22435-61-6)

Guidance literature:

Methyl-2,O³-dibenzoyl-4,6-dithiocyanato-4,6-didesoxy-α-D-galactopyranosid>, Raney-Ni;

DOI:10.1016/S0008-6215(00)81686-9

upstream raw materials:

carbon monoxide

C₂₁H₂₁IO₆

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