1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate

Base Information

• Chemical Name: 1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate
• CAS No.: 1018349-42-2
• Molecular Formula: CF₃O₃S*C₁₃H₁₃BrNO
• Molecular Weight: 428.227
• Mol file: 1018349-42-2.mol

Synonyms:1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate

Chemical Property of 1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of 1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate

There total 1 articles about 1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-(2-bromophenylmethoxy)pyridine (1018349-34-2) + methyl trifluoromethanesulfonate (333-27-7) → 1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate (1018349-42-2)

Guidance literature:

In toluene; at 0 - 20 ℃; for 1.5h;

DOI:10.1039/c5cc08488a

Reference yield:

1-methyl 2-(2-bromophenylmethyloxy)pyridinium trifluoromethanesulfonate (1018349-42-2) + (2,3,6-tri-O-methyl)-α,β-maltoheptaose → 1(I),4(VII)-O-bis(2-bromophenylmethyl)-2,3,6-O-trimethylmaltoheptaose + 1(I),4(VII)-O-bis(2-bromophenylmethyl)-2,3,6-O-trimethylmaltoheptaose

Guidance literature:

With magnesium oxide; for 48h; Overall yield = 30%; Overall yield = 0.31 g; Reflux; Inert atmosphere;

DOI:10.1039/c5cc08488a

upstream raw materials:

2-(2-bromophenylmethoxy)pyridine

methyl trifluoromethanesulfonate