(+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester)

Base Information

• Chemical Name: (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester)
• CAS No.: 108595-93-3
• Molecular Formula: C₆H₁₀BrNO₂
• Molecular Weight: 208.055
• Mol file: 108595-93-3.mol

Synonyms:(+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester)

Chemical Property of (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester)

There total 3 articles about (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexene (110-83-8) → (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester) (108595-93-3) + dimethyl sulfoxide (67-68-5,8070-53-9)

Guidance literature:

With chloroform;

DOI:10.1002/zaac.19572900103

Reference yield:

2-bromocyclocyclohexanol (2425-33-4,16536-57-5,24796-87-0,53023-24-8,53023-25-9,60933-67-7,5537-67-7) → (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester) (108595-93-3)

Guidance literature:

With sulfuric acid; sodium nitrite; unter Kuehlung;

DOI:10.1039/jr9360000285

Reference yield:

cyclohexene (110-83-8) → (+/-)-nitrous acid-(trans-2-bromo-cyclohexyl ester) (108595-93-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous HOBr solution

2: aqueous H₂SO₄; NaNO₂ / unter Kuehlung

With sulfuric acid; hypobromous acid; sodium nitrite;

DOI:10.1039/jr9360000285

upstream raw materials:

2-bromocyclocyclohexanol

cyclohexene