P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

Base Information

Chemical Name:P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene
CAS No.:252202-12-3
Molecular Formula:C₂₀H₁₇F₃O₃S
Molecular Weight:394.414
Hs Code.:

Synonyms:P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

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Chemical Property of P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

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Technology Process of P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

There total 2 articles about P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 252202-11-2
P-1-(4',6'-dimethyl-2'-hydroxyphenyl)-2-methylnaphthalene

: 252202-12-3
P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/S0957-4166(99)00299-2

Reference yield:

: 2-(2-bromomethyl-naphthalen-1-yl)-3,5-dimethyl-phenol

: 252202-12-3
P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

2: 98 percent / DABCO / CH₂Cl₂ / 0.5 h / 0 °C

With 1,4-diaza-bicyclo[2.2.2]octane; lithium aluminium tetrahydride; In diethyl ether; dichloromethane; 1: Reduction / 2: triflation;
DOI:10.1016/S0957-4166(99)00299-2

Reference yield: 86.0%

: 4559-70-0
Diphenylphosphine oxide

: 252202-12-3
P-1-(4',6'-dimethyl-2'-trifluoromethylsulfonyloxyphenyl)-2-methylnaphthalene

: 252202-13-4
P-1-(4',6'-dimethyl-2'-diphenylphosphanylphenyl)-2-methylnaphthalene

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In dimethyl sulfoxide; at 100 ℃; for 6h;
DOI:10.1016/S0957-4166(99)00299-2