Technology Process of C28H38N2O6S
There total 6 articles about C28H38N2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C
2: sodium tetrahydroborate; sodium acetate; acetic acid / methanol / 0.5 h / 20 °C
3: triethylamine / dichloromethane / 1 h / 20 °C
4: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; sodium acetate; sodium hydride; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / 0 °C
1.2: 4 h / 0 °C
2.1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h / 20 °C
3.1: sodium tetrahydroborate; sodium acetate; acetic acid / methanol / 0.5 h / 20 °C
4.1: triethylamine / dichloromethane / 1 h / 20 °C
5.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C
With
sodium tetrahydroborate; hydrogen; sodium acetate; chloroformic acid ethyl ester; sodium hydride; acetic acid; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; mineral oil;
