(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

Base Information

Chemical Name:(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole
CAS No.:34293-63-5
Molecular Formula:C₁₅H₁₁N₇O₄
Molecular Weight:353.297
Hs Code.:

Synonyms:(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

Chemical Property:

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Technology Process of (E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

There total 5 articles about (E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34296-51-0
1-phenyl-1,2,3-triazole-4-carbaldehyde

: 76195-86-3,55907-61-4
2,4-dinitrophenylhydrazine hydrochloride

: 34293-63-5
(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

Guidance literature:: With sulfuric acid; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2013.12.039

Reference yield:

: 62-53-3
aniline

: 34293-63-5
(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C

1.2: 1 h / 0 - 5 °C

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

4.1: sulfuric acid / ethanol / 24 h / 20 °C

With hydrogenchloride; copper(ll) sulfate pentahydrate; sulfuric acid; sodium L-ascorbate; sodium nitrite; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2013.12.039

Reference yield:

: 622-37-7
Phenyl azide

: 34293-63-5
(E)-4-((2-(2,4-dinitrophenyl)hydrazono)methyl)-1-phenyl-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

3: sulfuric acid / ethanol / 24 h / 20 °C

With copper(ll) sulfate pentahydrate; sulfuric acid; sodium L-ascorbate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2013.12.039