Technology Process of C20H25NO4S
There total 6 articles about C20H25NO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-ethylidene-1-(4-methylbenzyl)azetidine; toluene-4-sulfonic acid;
In
dichloromethane;
at 20 ℃;
for 0.166667h;
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 15h;
Reflux;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: bromine / dichloromethane / 2.5 h / 0 - 20 °C
2.1: titanium tetrachloride; triethylamine / diethyl ether / 15 h / 0 - 20 °C
3.1: sodium tetrahydroborate / methanol / 20 °C
4.1: acetonitrile / 15 h / Reflux
5.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 120 °C / Microwave irradiation
6.1: dichloromethane / 0.17 h / 20 °C
6.2: 15 h / Reflux
With
sodium tetrahydroborate; potassium tert-butylate; bromine; titanium tetrachloride; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: acetonitrile / 15 h / Reflux
2.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 120 °C / Microwave irradiation
3.1: dichloromethane / 0.17 h / 20 °C
3.2: 15 h / Reflux
With
potassium tert-butylate;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340250