Technology Process of C25H25NO7S2
There total 4 articles about C25H25NO7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 - 40 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium methylate / dimethyl sulfoxide; tetrahydrofuran / 3 h / 50 °C / Inert atmosphere
2: hydroxylamine hydrochloride; sodium hydroxide / N,N-dimethyl-formamide; water / 29 - 40 °C / Inert atmosphere
3: triethylamine / N,N-dimethyl-formamide / 20 - 40 °C / Inert atmosphere
With
hydroxylamine hydrochloride; sodium methylate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,4-diaza-bicyclo[2.2.2]octane / dimethyl sulfoxide / 20 - 28 °C / Inert atmosphere
2: sodium methylate / dimethyl sulfoxide; tetrahydrofuran / 3 h / 50 °C / Inert atmosphere
3: hydroxylamine hydrochloride; sodium hydroxide / N,N-dimethyl-formamide; water / 29 - 40 °C / Inert atmosphere
4: triethylamine / N,N-dimethyl-formamide / 20 - 40 °C / Inert atmosphere
With
1,4-diaza-bicyclo[2.2.2]octane; hydroxylamine hydrochloride; sodium methylate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;