1-(2-Bromoethyl)-2,3-difluorobenzene

Base Information

Chemical Name:1-(2-Bromoethyl)-2,3-difluorobenzene
CAS No.:126163-29-9
Molecular Formula:C₈H₇BrF₂
Molecular Weight:221.044
Hs Code.:
European Community (EC) Number:870-015-2

Synonyms:1-(2-bromoethyl)-2,3-difluorobenzene;126163-29-9;2,3-difluorophenethyl bromide;SCHEMBL3121976;SWRNHMXIOFDOLQ-UHFFFAOYSA-N;BFA16329;AKOS013305117;AB92779;C77832;EN300-132679

Suppliers and Price of 1-(2-Bromoethyl)-2,3-difluorobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3-Difluorophenethylbromide
10mg
$ 45.00

AK Scientific
1-(2-Bromoethyl)-2,3-difluorobenzene
100mg
$ 328.00

Acrotein
2,3-Difluorophenethylbromide 97%
5g
$ 440.00

ACHEMBLOCK
2,3-Difluorophenethylbromide 95%
5G
$ 540.00

ACHEMBLOCK
2,3-Difluorophenethylbromide 95%
1G
$ 190.00

Total 2 raw suppliers

Chemical Property of 1-(2-Bromoethyl)-2,3-difluorobenzene

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:219.96992
Heavy Atom Count:11
Complexity:119

Purity/Quality:

95%-98% ^*data from raw suppliers

2,3-Difluorophenethylbromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)F)F)CCBr

Technology Process of 1-(2-Bromoethyl)-2,3-difluorobenzene

There total 4 articles about 1-(2-Bromoethyl)-2,3-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1239331-90-8
(2,3-difluorophenyl)-ethyl 4-methylbenzenesulfonate

: 126163-29-9
1-(2-bromoethyl)-2,3-difluorobenzene

Guidance literature:: With lithium bromide; In acetone; for 3h; Reflux;
DOI:10.1021/jm3007933

Reference yield: 89.0%

: 126163-30-2
2-(2,3-difluorophenyl)ethanol

: 126163-29-9
1-(2-bromoethyl)-2,3-difluorobenzene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 145689-41-4
2-(2,3-difluorophenyl)acetic acid

: 126163-29-9
1-(2-bromoethyl)-2,3-difluorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / Reflux

1.2: 1 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 5 h / 20 °C

3.1: lithium bromide / acetone / 3 h / Reflux

With dimethylsulfide borane complex; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jm3007933