((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

Base Information

Chemical Name:((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)
CAS No.:85763-88-8
Molecular Formula:C₄₂H₃₂N₄O₂P₂PdRh*ClO₄
Molecular Weight:995.465
Hs Code.:

Synonyms:((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

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Technology Process of ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

There total 1 articles about ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 85751-22-0
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

: 85763-88-8
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

Guidance literature:: With carbon monoxide; In dichloromethane; CO bubbled through CH2Cl2 soln. ((dpe)Pd(μ-BiBzIm)Rh(COD))(ClO4) at atmospheric pressure for 20 min; soln. evapd. partially, ether added; elem. anal.;
DOI:10.1016/S0277-5387(00)83951-0

Reference yield: 91.0%

: 85763-88-8
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

: 85744-59-8
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)(PPh3))(ClO4)

Guidance literature:: With triphenylphosphine; In dichloromethane; byproducts: CO; equimolecular mixt. ((dpe)Pd(μ-BiBzIm)Rh(CO)2)(ClO4) and PPh3 in CH2Cl2 stirred at room temp. for 2 h; soln. evapd. partially, hexane added; elem. anal.;
DOI:10.1016/S0277-5387(00)83951-0