((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

Base Information

Chemical Name:((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)
CAS No.:85751-22-0
Molecular Formula:C₄₈H₄₄N₄P₂PdRh*ClO₄
Molecular Weight:1047.63
Hs Code.:

Synonyms:((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

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Chemical Property of ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

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Technology Process of ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

There total 1 articles about ((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 85744-47-4
Pd(bibenzimidazolate)(1,2-bis-(diphenylphosphino)ethane)

: silver perchlorate

: 85751-22-0
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

: silver(I) chloride

Guidance literature:: In dichloromethane; acetone; mixt. (Rh(μ-Cl)(COD))2, AgClO4 and Pd(BiBzIm)(dpe) in CH2Cl2-Me2CO (1:1) stirred at room temp. for 20 min; AgCl filtered off, filtrate evapd., ether added; elem. anal.;
DOI:10.1016/S0277-5387(00)83951-0

Reference yield: 92.0%

: 85751-22-0
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(1,5-cyclooctadiene))(ClO4)

: 85763-88-8
((1,2-bis(diphenylphosphino)ethane)Pd(μ-bibenzimidazolate)Rh(CO)2)(ClO4)

Guidance literature:: With carbon monoxide; In dichloromethane; CO bubbled through CH2Cl2 soln. ((dpe)Pd(μ-BiBzIm)Rh(COD))(ClO4) at atmospheric pressure for 20 min; soln. evapd. partially, ether added; elem. anal.;
DOI:10.1016/S0277-5387(00)83951-0