S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

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Chemical Name:S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate
CAS No.:102437-86-5
Molecular Formula:C₂₄H₂₈N₂O₅S₂
Molecular Weight:488.629
Hs Code.:

Synonyms:S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

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Chemical Property of S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

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Technology Process of S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

There total 4 articles about S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.6%

: 68563-70-2
cis-2-methyl-N-phenyl-1,3-oxathiolane-2-acetamide 3-oxide

: 102437-86-5
S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

Guidance literature:: In N,N-dimethyl-formamide; benzene; at 50 ℃; for 5h;
DOI:10.1021/jo00364a033

Reference yield:

: 102437-91-2
(E)-3-{2-[2-((E)-1-Methyl-2-phenylcarbamoyl-vinyloxy)-ethyldisulfanyl]-ethoxy}-but-2-enoic acid phenylamide

: 102437-86-5
S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 ℃; for 0.05h;
DOI:10.1021/jo00364a033

Reference yield:

: 102-01-2,98624-45-4
N-phenylacetoacetamide

: 102437-86-5
S-<2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethyl> 2-<<1-methyl-3-oxo-3-(phenylamino)-1-propenyl>oxy>ethanethiosulfinate

Guidance literature:: Multi-step reaction with 3 steps

1: 90.2 percent / p-toluenesulfonic acid monohydrate (PTSA) / benzene / 5 h / Heating

2: 0.4968 g / 35percent aq. H₂O₂, acetic acid / 1 h / 15 - 20 °C

3: 59.6 percent / benzene; dimethylformamide / 5 h / 50 °C

With dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00364a033