methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Base Information

Chemical Name:methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)
CAS No.:80471-11-0
Molecular Formula:C₄₅H₃₉IIr₂N₄O₂P₂
Molecular Weight:1241.12
Hs Code.:

Synonyms:methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

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Chemical Property of methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

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Technology Process of methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

There total 3 articles about methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 80471-11-0
methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: With CH₃I; In tetrahydrofuran; diethyl ether; under N2, soln. of MeI (1 equiv or excess) in Et2O was added dropwise to stirred soln. of Ir-complex in THF over 2 min; concd., hexane added, cooled slowly to -25°C; elem. anal.;

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 80471-11-0
methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: CH₃I / tetrahydrofuran; diethyl ether

With CH₃I; In tetrahydrofuran; diethyl ether;

Reference yield:

: 101010-16-6
{Ir2(μ-η2-pyrazolate)2(η4-1,4-cyclooctadiene)2}

: 80471-11-0
methyldicarbonyliodobis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(II)

Guidance literature:: Multi-step reaction with 2 steps

1: CO; triphenylphosphine / tetrahydrofuran

2: CH₃I / tetrahydrofuran; diethyl ether

With CO; triphenylphosphine; CH₃I; In tetrahydrofuran; diethyl ether;