rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

Base Information

Chemical Name:rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)
CAS No.:870633-97-9
Molecular Formula:C₅₉H₉₃N₃O₅S
Molecular Weight:956.471
Hs Code.:

Synonyms:rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

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Chemical Property of rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

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Technology Process of rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

There total 4 articles about rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27144-18-9
3-(tritylthio) propanoic acid

: 870633-97-9
rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 2-ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline / 1,2-dichloro-ethane / 16 h / Heating

2: 4-dimethylaminopyridine / tetrahydrofuran / 3 h / 20 °C

3: tetrahydrofuran / 48 h / 20 °C

With dmap; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/j.chemphyslip.2005.03.006

Reference yield:

: 850416-23-8
rac-3-(tritylsulfanyl)-N-(2,3-dihydroxypropyl)propanamide

: 870633-97-9
rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

Guidance literature:: Multi-step reaction with 2 steps

1: 4-dimethylaminopyridine / tetrahydrofuran / 3 h / 20 °C

2: tetrahydrofuran / 48 h / 20 °C

With dmap; In tetrahydrofuran;
DOI:10.1016/j.chemphyslip.2005.03.006

Reference yield:

: 76-83-5
trityl chloride

: 870633-97-9
rac-3-{[3-(tritylsulfanyl)propanoyl]amino}propane-1,2-diyl bis(hexadecylcarbamate)

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / CH₂Cl₂ / 16 h / 20 °C

2: 87 percent / 2-ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline / 1,2-dichloro-ethane / 16 h / Heating

3: 4-dimethylaminopyridine / tetrahydrofuran / 3 h / 20 °C

4: tetrahydrofuran / 48 h / 20 °C

With dmap; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.chemphyslip.2005.03.006