butyl[(5-methylfuran-2-yl)methyl]amine

Base Information

• Chemical Name: butyl[(5-methylfuran-2-yl)methyl]amine
• CAS No.: 130539-97-8
• Molecular Formula: C₁₀H₁₇NO
• Molecular Weight: 167.251
• Mol file: 130539-97-8.mol

Synonyms:N-(5-methylfurfuryl)-n-butylamine

Chemical Property of butyl[(5-methylfuran-2-yl)methyl]amine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

BUTYL[(5-METHYLFURAN-2-YL)METHYL]AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of butyl[(5-methylfuran-2-yl)methyl]amine

There total 5 articles about butyl[(5-methylfuran-2-yl)methyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2-methylfuran (534-22-5) + N-<(Benzotriazolyl)methyl>butylamine (142920-55-6) → N-(5-methylfurfuryl)-n-butylamine (130539-97-8)

Guidance literature:

With zinc(II) chloride; In dichloromethane; for 3h; Heating;

DOI:10.1016/S0040-4020(01)81590-8

Reference yield: 13.0%

2-methylfuran (534-22-5) → N-(5-methylfurfuryl)-n-butylamine (130539-97-8) + N,N-di(5-methylfurfuryl)-n-butylamine (130539-96-7)

Guidance literature:

In acetonitrile; for 22h; Ambient temperature;

DOI:10.1016/S0040-4039(00)97589-0

Reference yield: 13.0%

2-methylfuran (534-22-5) + Butyl-ethoxymethyl-methylene-ammonium; chloride → N-(5-methylfurfuryl)-n-butylamine (130539-97-8) + N,N-di(5-methylfurfuryl)-n-butylamine (130539-96-7)

Guidance literature:

In acetonitrile; for 22h; Ambient temperature;

DOI:10.1016/0040-4020(96)00026-9

upstream raw materials:

2-methylfuran

n-butylamine hydrochloride

N-<(Benzotriazolyl)methyl>butylamine

5-Methylfurfural

Refernces

• 1、 Heaney, Harry,Papageorgiou, George. "The use of bis(aminol) ethers derived from aliphatic primary amines in the synthesis of secondary and tertiary amines". . p. 3473 - 3486. Retrieved 2007/10/03.
• 2、 Earle, Martyn J.,Fairhurst, Robin A.,Heaney, Harry,Papageorgiou, George,Wilkins, Robert F.. "A new route to secondary amines from bis-(alkoxymethyl)-alkylamines - The activation of an aminomethyl group and protection of the product by the same functional group". . p. 4229 - 4232. Retrieved 2007/10/02.