(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

Base Information

Chemical Name:(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester
CAS No.:92598-82-8
Molecular Formula:C₁₈H₂₄N₂O₃
Molecular Weight:316.4
Hs Code.:

Synonyms:(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

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Technology Process of (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

There total 1 articles about (2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54-71-7
pilocarpine hydrochloride

: 92598-82-8
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / H₂O / 1 h / 0 - 4 °C

2: 35 percent / dimethylformamide / Ambient temperature

With sodium hydroxide; In water; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600750109

Reference yield:

: 92598-82-8
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

: 92-13-7
pilocarpine

Guidance literature:: With phosphate buffer; at 37 ℃; Rate constant; pH 7.40;
DOI:10.1002/jps.2600750109

Reference yield:

: 10400-19-8
3-pyridinecarbonyl chloride

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 92598-82-8
(2S,3R)-2-Ethyl-3-hydroxymethyl-4-(3-methyl-3H-imidazol-4-yl)-butyric acid benzyl ester

: Nicotinic acid (2R,3S)-3-benzyloxycarbonyl-2-(3-methyl-3H-imidazol-4-ylmethyl)-pentyl ester; compound with (E)-but-2-enedioic acid

Guidance literature:: With sodium hydrogencarbonate; potassium carbonate; Yield given. Multistep reaction; 1.) toluene, RT, 3 h, 2.) ether, 2-propanol;
DOI:10.1002/jps.2600750811