(E)-3-chloro-β-iodostyrene

Base Information

Chemical Name:(E)-3-chloro-β-iodostyrene
CAS No.:1381775-28-5
Molecular Formula:C₈H₆ClI
Molecular Weight:264.493
Hs Code.:

Synonyms:(E)-3-chloro-β-iodostyrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-chloro-β-iodostyrene

Chemical Property:

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Technology Process of (E)-3-chloro-β-iodostyrene

There total 3 articles about (E)-3-chloro-β-iodostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 115665-71-9
(E)-1-(2-bromovinyl)-3-chlorobenzene

: 1381775-28-5
(E)-3-chloro-β-iodostyrene

Guidance literature:: With copper(I) oxide; L-proline; potassium iodide; In ethanol; at 110 ℃; for 24h; diastereospecific reaction; Schlenk technique; Sealed tube; Inert atmosphere; Green chemistry;
DOI:10.1055/s-0036-1588988

Reference yield:

: 1866-38-2,14473-90-6
3-chlorocinnamic acid

: 1381775-28-5
(E)-3-chloro-β-iodostyrene

Guidance literature:: 3-chlorocinnamic acid; With lithium acetate; In water; acetonitrile; at 20 ℃; for 0.0833333h;

With N-iodo-succinimide; In water; acetonitrile; at 20 ℃;
DOI:10.1016/j.tet.2012.04.048

Reference yield:

: 3020-28-8
(iodomethyl)triphenylphosphonium iodide

: 587-04-2
m-Chlorobenzaldehyde

: 1381775-28-5
(E)-3-chloro-β-iodostyrene

: (Z)-1-chloro-3-(2-iodovinyl)benzene

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 1h; Overall yield = 67percent; Overall yield = 633 mg; Inert atmosphere;
DOI:10.1021/acs.orglett.9b02540