10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Base Information

Chemical Name:10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one
CAS No.:1370410-54-0
Molecular Formula:C₂₃H₁₇NO₂
Molecular Weight:339.393
Hs Code.:

Synonyms:10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

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Chemical Property of 10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

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Technology Process of 10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

There total 5 articles about 10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2749-94-2
1-methoxy-4-(prop-1-yn-1-yl)benzene

: 202132-25-0
2-bromo-N-(2-iodophenyl)benzamide

: 1370410-54-0
10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; lithium chloride; In N,N-dimethyl-formamide; at 120 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1039/c9cc03566d

Reference yield: 98.0%

: 1370410-23-3
C₂₃H₁₈INO₂

: 1370410-54-0
10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Guidance literature:: With sodium phosphate dibasic dodecahydrate; silver(I) acetate; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1021/ol300584m

Reference yield:

: 5782-15-0
2-(4-methoxyphenyl)-3-methyl-1H-indole

: 1370410-54-0
10b-(4-methoxyphenyl)-11-methylene-10b,11-dihydro-6H-isoindolo[2,1-a]indol-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 20 - 70 °C

2: sodium phosphate dibasic dodecahydrate; silver(I) acetate; palladium diacetate / N,N-dimethyl-formamide / 12 h / 80 °C

With sodium phosphate dibasic dodecahydrate; silver(I) acetate; palladium diacetate; sodium hydride; In N,N-dimethyl-formamide; 2: Heck reaction;
DOI:10.1021/ol300584m