Technology Process of C27H26N2O6
There total 7 articles about C27H26N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon;
In
methanol;
for 12h;
under 30003 Torr;
DOI:10.1021/jm300985d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C
2.1: oxalyl dichloride / tetrahydrofuran / 0.5 h / 0 °C
3.1: triethylamine / tetrahydrofuran / 0 °C
3.2: 0 - 20 °C
4.1: palladium 10% on activated carbon / methanol / 12 h / 30003 Torr
With
oxalyl dichloride; palladium 10% on activated carbon; water; triethylamine; lithium hydroxide;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm300985d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / tetrahydrofuran / 0.5 h / 0 °C
2.1: triethylamine / tetrahydrofuran / 0 °C
2.2: 0 - 20 °C
3.1: palladium 10% on activated carbon / methanol / 12 h / 30003 Torr
With
oxalyl dichloride; palladium 10% on activated carbon; triethylamine;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm300985d