di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

Base Information

Chemical Name:di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene
CAS No.:656256-40-5
Molecular Formula:C₂₄H₂₃N₅O
Molecular Weight:397.48
Hs Code.:

Synonyms:di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

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Chemical Property of di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

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Technology Process of di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

There total 2 articles about di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 28188-41-2
m-(bromomethyl)benzonitrile

: 656256-35-8
2-methylphenyl bis(1-methyl-2-imidazolyl) methanol

: 656256-40-5
di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

Guidance literature:: 2-methylphenyl bis(1-methyl-2-imidazolyl) methanol; With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.166667h;

m-(bromomethyl)benzonitrile; In dimethyl sulfoxide; at 20 ℃; for 5h; Further stages.;
DOI:10.1002/chem.200390082

Reference yield:

: 87-24-1
ethyl 2-methylbenzoate

: 656256-40-5
di(1-methyl-2-imidazolyl)(3-cyanobenzyloxy)methyl-2-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: nBuLi / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 72 percent / hexane; tetrahydrofuran / -78 - 20 °C

2.1: KOH / dimethylsulfoxide / 0.17 h / 20 °C

2.2: 85 percent / dimethylsulfoxide / 5 h / 20 °C

With potassium hydroxide; n-butyllithium; In tetrahydrofuran; hexane; dimethyl sulfoxide;
DOI:10.1002/chem.200390082