1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

Base Information

Chemical Name:1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane
CAS No.:1629864-87-4
Molecular Formula:C₁₉H₂₆O₅
Molecular Weight:334.412
Hs Code.:

Synonyms:1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

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Chemical Property of 1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

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Technology Process of 1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

There total 3 articles about 1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1629864-84-1
1-[4-(4-methoxyphenoxy)]butyl zinc iodide

: 34819-86-8
3,4-di-O-acetyl-6-deoxy-L-glucal

: 1629864-86-3
1-C-(4-O-acetyl-2,3,6-trideoxy-α-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

: 1629864-87-4
1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 - 15 ℃; for 48h; Sealed tube;
DOI:10.3390/molecules19067072

Reference yield:

: 150-76-5
4-methoxy-phenol

: 1629864-86-3
1-C-(4-O-acetyl-2,3,6-trideoxy-α-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

: 1629864-87-4
1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; tetrabutyl ammonium fluoride / water; dichloromethane / 24 h

2.1: sodium iodide / acetone / 20 °C

3.1: tetrahydrofuran; ethylene dibromide / 0.17 h / 56 °C

3.2: 0.25 h / 20 °C

3.3: 0.75 h / 20 °C

4.1: boron trifluoride diethyl etherate / dichloromethane / 48 h / -30 - 15 °C / Sealed tube

With boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; ethylene dibromide; acetone;
DOI:10.3390/molecules19067072

Reference yield:

: 2033-83-2
1-(4-methoxyphenoxy)-4-bromobutane

: 1629864-86-3
1-C-(4-O-acetyl-2,3,6-trideoxy-α-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

: 1629864-87-4
1-C-(4-O-acetyl-2,3,6-trideoxy-β-L-erythro-hex-2-enopyranosyl)-4-(4'-methoxyphenoxy)butane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / acetone / 20 °C

2.1: tetrahydrofuran; ethylene dibromide / 0.17 h / 56 °C

2.2: 0.25 h / 20 °C

2.3: 0.75 h / 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / 48 h / -30 - 15 °C / Sealed tube

With boron trifluoride diethyl etherate; sodium iodide; In tetrahydrofuran; dichloromethane; ethylene dibromide; acetone;
DOI:10.3390/molecules19067072