Technology Process of C38H47F2N3O5
There total 8 articles about C38H47F2N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide) / 3 h
2: 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
With
3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine;
In
DMF (N,N-dimethyl-formamide);
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / 2 h / -20 - 0 °C
1.2: -78 °C
2.1: lithium hydroxide; dihydrogen peroxide / tetrahydrofuran; water / 8 h / 0 °C
3.1: diphenyl phosphoryl azide; triethylamine / toluene / 4 h / 20 - 80 °C
4.1: lithium hydroxide / ethanol; water / 4 h / 85 °C
5.1: 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
With
lithium hydroxide; di-n-butylboryl trifluoromethanesulfonate; diphenyl phosphoryl azide; dihydrogen peroxide; 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide / ethanol; water / 4 h / 85 °C
2: 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine / DMF (N,N-dimethyl-formamide) / 18 h / 20 °C
With
lithium hydroxide; 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; benzotriazol-1-ol; triethylamine;
In
DMF (N,N-dimethyl-formamide); ethanol; water;