1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

Base Information

Chemical Name:1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane
CAS No.:1439809-15-0
Molecular Formula:C₂₈H₃₀N₄P₂
Molecular Weight:484.521
Hs Code.:

Synonyms:1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

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Chemical Property of 1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

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Technology Process of 1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

There total 4 articles about 1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-pyridinium methylsulfate

: 1439809-15-0
1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium / diethyl ether / 48 h / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

3.1: 110 °C / Inert atmosphere

4.1: ethanol / 0.5 h / 20 °C

With lithium aluminium tetrahydride; sodium; In diethyl ether; ethanol;
DOI:10.1002/chem.201304234

Reference yield:

: 23081-78-9
diethyl pyridin-2-yl-2-phosphonate

: 1439809-15-0
1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere

2: 110 °C / Inert atmosphere

3: ethanol / 0.5 h / 20 °C

With lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1002/chem.201304234

Reference yield:

: 125995-76-8
pyridin-2-ylphosphine

: 1439809-15-0
1,5-bis(p-tolyl)-3,7-bis(pyridine-2-yl)-1,5-diaza-3,7-diphosphacyclooctane

Guidance literature:: Multi-step reaction with 2 steps

1: 110 °C / Inert atmosphere

2: ethanol / 0.5 h / 20 °C

In ethanol;
DOI:10.1002/chem.201304234