10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

Base Information

Chemical Name:10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride
CAS No.:1239018-78-0
Molecular Formula:C₂₄H₂₈FN₅O₇S
Molecular Weight:549.58
Hs Code.:

10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

Synonyms:10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

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Chemical Property of 10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

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Technology Process of 10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

There total 1 articles about 10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32833-96-8
N,N-dimethyloxamic acid

: 1239018-77-9
10-amino-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

: 1239018-78-0
10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1239018-78-0
10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride

: 1188424-93-2
N₁-(2-((4-fluorobenzyl)carbamoyl)-3-hydroxy-4-oxo-6,7,8,9-tetrahydro-7,10-ethanopyrimido[1,2-a]azepin-10(4H)-yl)-N,N-dimethyloxalamide

Guidance literature:: 10-((dimethylamino(oxo)acetyl)amino)-2-(4-fluorobenzylcarbamoyl)-4-oxo-4,6,7,8,9,10-hexahydro-7,10-ethanopyrimido[1,2-a]azepin-3-yl methanesulfonate hydrochloride; With water; sodium hydroxide; In isopropyl alcohol; at 20 ℃; for 1h;

With 1-hydroxy-1,1,2-ethanetricarboxylic acid; In water; ethyl acetate;