8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Base Information

Chemical Name:8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene
CAS No.:135128-68-6
Molecular Formula:C₂₂H₁₈N₄OS₂
Molecular Weight:418.543
Hs Code.:

Synonyms:8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Suppliers and Price of 8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

There total 5 articles about 8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 135128-66-4
6-(4-Ethoxy-phenyl)-4-(3-methyl-1-phenyl-5-thioxo-4,5-dihydro-1H-pyrazol-4-yl)-2H-pyridazine-3-thione

: 135128-68-6
8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Guidance literature:: With sodium hydroxide; iodine; potassium iodide; In water;
DOI:10.1246/bcsj.64.2032

Reference yield:

: 29582-31-8
(E)-4-(4-ethoxyphenyl)-4-oxobut-2-enoic acid

: 135128-68-6
8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / benzene / 10 h / Heating

2: 60 percent / hydrazine hydrate / ethanol / 5 h / Heating

3: 69 percent / P₂S₅ / xylene / 6 h / Heating

4: 76 percent / I₂, KI, NaOH / H₂O

With sodium hydroxide; tetraphosphorus decasulfide; iodine; hydrazine hydrate; potassium iodide; In ethanol; water; xylene; benzene;
DOI:10.1246/bcsj.64.2032

Reference yield:

: 135128-61-9
6-(p-Ethoxyphenyl)-4-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-4,5-dihydro-3(2H)-pyridazinone

: 135128-68-6
8-(4-Ethoxy-phenyl)-1-methyl-3-phenyl-3H-4,5-dithia-2,3,6,7-tetraaza-cyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / P₂S₅ / xylene / 6 h / Heating

2: 76 percent / I₂, KI, NaOH / H₂O

With sodium hydroxide; tetraphosphorus decasulfide; iodine; potassium iodide; In water; xylene;
DOI:10.1246/bcsj.64.2032